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Benefits of gas Purging (
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( back to section 1 )
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Homogenizes the melt
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Removes contaminants
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Regulates temperature
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Operational
requirements for a purging plug (
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( back to section 1 )
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Achieving Process Aims |
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Desulfurization (Turbulent Stir)
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Cleaning, Homogenization (Soft Stir) |
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Wear Resistance |
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Against Thermal Shocks
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Against Hot Erosion
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Infiltration Resistance |
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Against Steel
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Against Slag
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Operational Safety |
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Against Breakthrough
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During Start up
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Easy Maintenance |
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Plug & Block
... any size or
composition to meet your needs.
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Types of plugs we offer (
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( back to section 1 )
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Durastir ND
Plug (Non Directional)
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Durastir DP
Plug (Directional Plug)
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We are also
able to make plugs and blocks any size or composition to meet
your needs.
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We are also an
agency for Special Shapes Refractory Co. which produces a plug
called the stirpro

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Wear
Mechanisms (
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( back to section 1 )
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Physical wear |
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erosion back attack
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spalling of infiltrated layers
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spalling by thermal shock
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Chemical wear |
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infiltration of slag
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infiltration of oxide phases
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infiltration of steel
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mineral transformation depending on the redox potential
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Wear parameter of ladle purging plugs (
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- Quantity of gas
- Pressure of gas
- Purging time
- Steel Quality (Viscosity)
- Steel Temperature
- Purging plug maintenance
(Purification with O2)
- Bottom Lining Life
- Purging Plug Type
- Ladle Circulation (Thermal Shocks)
- Infiltrations
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Ladle
refining station (
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( back to section 1 )

Final Alloying
Desulfurization
Oxygen / Hydrogen removal
Reheating
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Oxygen
removal - Porous plug (
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( back to section 1 )

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- DEOXIDIZING CONDITIONS
- Si-Mn DEOXIDATION INSIDE
FURNACE: Si0.5 –0.8 % Mn1.2 –1.7 %
- AL DEOXIDATION (AL 1.1 lbs/ton
ADDED INTO FURNACE)
- BASICITY OF SLAG 1.4-2.6
- ARGON PRESSURE 42.6 PSI
- ARGON FLOW 5SCFM
- INJECTION TIME 6 MIN. max
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Hydrogen
removal (
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- TYPE OF STEEL .35 C, .8MN
- 25 T HEAT SIZE
- TOTAL BUBBLING TIME –9 MINUTES
- GAS FLOW 75 SCFM
- GAS PRESSURE 55 PSI
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250 ton
ladle, diameter at top - 11.3 ft (
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( back to section 1 )

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Temperature
homogenization (
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( back to section 1 )

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- ABOVE GRAPH FOR 150 TON LADLE
- INJECTION TIME 12 MINUTES
- GAS FLOW 9 SCFM
- GAS PRESSURE 49.7 PSI
- WITH BUBBLING TEMPERATURE
STRATIFICATION WILL BE 50OF OR LESS
- WITHOUT BUBBLING TEMPERATURE
STRATIFICATION WILL BE 120OF OR MORE
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Standard CFM
needed for sulphur removal (
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( back to section 1 )

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Sulphur removal (
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( back to section 1 ) |
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BEARING QUALITY STEEL
225 TON PER HEAT
TAP TEM. 3000O*
LADLE TEMP. 2910O*
FINISH TEMP. 2800O*
*NO CAL-SIL INJECTION
SULPHUR AT START 0.032
SULFUR AT FINISH 0.011
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*USED SYNTHETIC TOP SLAG
80% BURNT LIME
20% FLOURSPAR
25 lbs. TON
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(
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Bottom of
ladle (
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( back to section 2 )

Plug location = radius / 2
Measured after refractory lining is in
place
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Position -
Pattern - Dead zones (
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( back to section 2 )


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Typical ladle
temperature profile (
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( back to section 2 )

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Stir plug
operating procedure (
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( back to section 3 )
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Do not apply
gas pressure to the plug exceeding 150psi.
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Establish flow
meter and back pressure reference points for your particular
operation.
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Perform a
natural gas check to determine the operational readiness of
the plug immediately after casting. See attached recommended
procedure.
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Between heats
and after degassing, look for the safety shape change feature
which will indicate when it is time for plug replacement.
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In conjunction
with the safety shape change feature, the life of the plug
should be determined by accurately recording the number of
stirring minutes on that particular plug. (Determining the
life of a plug by the number of heats could be misleading and
is not recommended.)
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Best stirring
practices do not break the slag cover. If a violent stirring
practice is followed, as sometimes with desulfurizing,
temperature control or vacuum degassing, follow-up with a soft
stir without breaking the slag cover in order to remove
impurities.
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The major
causes resulting in no stirs are:
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Schematic
setup of the flow control panel at the steel plant (
back to top )
( back to section 3 )

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Comparative
table for gases (
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( back to section 3 )
Gas
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Nitrogen |
Argon |
Carbon Dioxide |
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Molecular Weight |
28.01 |
39.94 |
44.01 |
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Specific Gravity Compared
with Air |
0.097 |
1.38 |
1.53 |
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Relative Cost |
1.00 |
6.67 |
0.77 |
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Theoretical
Argon gas pressure versus ladle height (
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( back to section 3 )

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(
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Gunning mix
protection for replacement plug (
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( back to section 4 )

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Seating block
and pocket block (
back to top )
( back to section 4 )

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(
back to top )
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What to check
when the plug does not work (
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( back to section 5 )
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Was the plug pretested for gas flow?
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Skull covering plug?
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Leaks in gas supply line?
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Check valve stuck in closed position?
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Weak bubble?
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Bypass gas valve left open?
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Raw material additions piled on plug?
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Is there solidified aluminum in the plug pipe?
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Is the plug covered with gunning refractory?
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Is there dirt, oil, water, etc. in the gas supply line?
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The reason
for the plug failure cannot be found ...
Remove the plug and check the following: (
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( back to section 5 )
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Ruptured casing
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Was it caused by using excessive gas pressure above 150psi?
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Steel / slag penetration
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Was it caused by oxygen lancing?
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Was slag forming additions, cal-sil, ferro silicon or aluminum
added directly onto the ladle bottom?
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Plug should be sectioned to observe for penetration.
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Pipe sizing
and obstructions (
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( back to section 5 )
Another common problem for gas purging are obstructions or kinks
in the lines. Although these seldom affect the line pressure
they can dramatically affect the volume or flow of gas to the
vessel.
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Pipe sizing
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Bends and turns
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Long runs
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Hose reels
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Quick disconnects
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Check valves
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GENERAL
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Use common sense and follow the system
from beginning to end. Do not enter closed gas-containing
spaces without proper safety equipment, i.e. sniffers, etc.
Inert gasses are odorless and can be very deadly.
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Pipe sizing
and obstructions (
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( back to section 5 )
These are placed in plugs to tell when the useful or safe life
of the plug has been used. Do not ignore these warnings. Always
remember – WHEN IN DOUBT -TAKE IT OUT! Either take the
ladle out of service, change the plug, or gun over the plug, but
do not use a plug that has worn to the indicator.
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Block repair
and maintenance (
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( back to section 5 )
As
a rule, blocks that have worn to ½ the length of the plug should
be replaced. Replacement plugs should be gunned up level with
the floor immediately after installation. Minor cracks should be
repaired from the cold face before installing the plug. Again,
do not take chances. If you doubt the integrity of the block,
take it out.
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Leaking
fittings and connections (
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( back to section 5 )
One
of the most common problems found in gas purging are leaks which
waste expensive gas, lead to weak or no stirs, and can create a
venturi effect, clogging off the plug completely. While welded
connections are preferred, this is not always possible, so the
system should be checked periodically for leaks.
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One way is to listen
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The fittings can be soap tested, or one could use his
hand to run over the connection to feel for leaks. Again, this
works best for the high pressure gasses, and is not usually
practical because of the time constraints.
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Odor
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Bag Test
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Many mills use this to immediately
show them if they have leaks. After the face of the plug is
lanced and opened, a flame is then run along the piping
while connected to the gas supply. A flame will indicate
where there are leaks. All leaks should be eliminated as
quickly as practical to save gas and insure stir
performance. Some people actually use lit bags, others use
rosebuds or torches, and others use lit rags on the end of
an old lance pipe. If this method is used, it should only
be used where the ladle is clearly accessible, and never in
a pit or closed-in area. As always, safety equipment,
including face shields, should be worn.
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GENERAL
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Checking the
plug (
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( back to section 5 )
To
achieve 100% stir performance a plug should be checked after
each cast flow. Different plants use different methods to
achieve the same goal.
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Back pressure
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Bubble gauges
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Flame test
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GENERAL
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Brushing the
plug (
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( back to section 5 )
If
the plug does not show flow, it may not stir with the next
heat. One option is to change the plug but this is not always
feasible. The second option is to brush the plug.
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Nitrogen
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Natural gas
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Gradall
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GENERAL
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When brushing a plug, try to stay
12”or more off the hot face of the plug and use a sweeping
or brushing pattern. Oxygen is usually at very high
pressures and will clog the plugs and prematurely wear out
refractories if held too close. Always wear protective
clothing and equipment when performing this function.
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Checking the
operational readiness of the porous plug after completion of
casting
(
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( back to section 5 )
After each casting, the operational readiness of the bubbling
system should be checked for the next service period.
Immediately after emptying the slag, natural gas or coke oven
gas is hooked up to the porous plug. There will be ignition
since the brick is still very hot. A flame indicates that gas
flow exists (Figure 1 below).
If
this is not the case, while leaving the gas in a turned on
position, the porous plug must be cleaned of slag and steel
residue from the inside of the ladle. This is done carefully
with an oxygen lance having a very soft flame (Figure 2 below).
A
black pipe with a 1” I.D. is recommended for the oxygen lance
when used to clean plugs installed in ladles 100 ton or larger.
For ladles 100 ton or smaller, a black pipe ½”– ¾” I.D. is
suggested. Applied oxygen pressure should range 70-100psi.
The
red glow will be seen during the period when the oxygen lance is
burning off solid metal. Once the metal covering the plug is
gone, the red will disappear and the color will turn dark or
black to indicate oxygen cleaning completion.
If
no gas flow can be achieved, the plug should be replaced.
Should the mentioned gas types not be available, it is possible
to run a check with argon or nitrogen. However, there will
become markedly darker in comparison to its surrounding. A heavy
shower of sparks will indicate renewed operational readiness.
Using compressed air may be risky since the oxygen content may
attack the steel casing.
The
gas flow test must be conducted carefully and accurately since
the service life and safety of the bubbling system will depend a
great deal on these work procedures. It is consequently
suggested that one employee per shift be assigned responsibility
for this work.
Gas purging cone pretest procedure

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Wear
mechanisms (
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( back to section 5 )

Bubble formatin (depending on purging gas quality)

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